27 October 1954 between August 1954 and May 1956, Joseph A. Walker, the National Advisory Committee for Aeronautics’ chief project test pilot for the Douglas X-3 supersonic research aircraft, made twenty research flights in the “Stiletto.” 
On the tenth flight, 27 October, Walker took the X-3 to an altitude of 30,000 feet (9,144 meters). With the rudder centered, he put the X-3 into abrupt left aileron rolls, first at 0.92 Mach and then at Mach 1.05. Both times, the aircraft violently yawed to the right and then pitched down. Walker was able to recover before the X-3 was completely out of control.
This was a new and little understood condition called inertial roll coupling. It was a result of the aircraft’s mass being concentrated within its fuselage, the gyroscopic effect of the turbojet engines and the inability of the wings and control surfaces to stabilize the airplane and overcome its rolling tendency. (Just two weeks earlier, North American Aviation’s Chief Test Pilot George S. Welch had been killed when the F-100A Super Sabre that he was testing also encountered inertial roll coupling and disintegrated.)
A post-flight inspection found that the X-3 had reached its maximum design load. The airplane was grounded for the next 11 months.
Source: ThisDayinAviation by Bryan R. Swopes